Heat treatment and surface

Case hardening (carburising, nitriding): what goes wrong and where to inspect

Gears, shafts and pins need a hard wear resistant surface over a tough core. Carburising, carbonitriding and nitriding diffuse carbon or nitrogen into the surface to achieve it.

01How the process works

In carburising, parts are heated in a carbon rich atmosphere so carbon diffuses into the surface, then quenched and tempered. Nitriding diffuses nitrogen at lower temperature without quenching, giving less distortion and a hard compound (white) layer.

Effective case depth, surface hardness and microstructure (retained austenite, carbides, white layer thickness) are the acceptance features. They are measured on sections of production parts or representative coupons in each load.

  1. Cleaning and masking. Parts cleaned; areas masked.
  2. Diffusion. Carburising or nitriding cycle.
  3. Quench. For carburised parts.
  4. Temper. Stress relief and hardness adjustment.
  5. Testing. Case depth traverse, hardness, microstructure.

02What typically goes wrong

DefectTypical causeHow it is found
Shallow or deep caseTime, temperature, carbon potentialHardness traverse
Low surface hardnessDecarburisation, retained austeniteMicrohardness, metallography
Excess white layerNitriding potentialMetallography
DistortionQuench, fixturingDimensional check
Soft spotsMasking, contaminationHardness survey
Grinding burn after case hardeningGrinding parametersNital etch

03Where an inspector should look

01

Before production

  • Case depth definition (e.g. 550 HV)
  • Coupon arrangement
  • Masking requirements
02

During production

  • Atmosphere control records
  • Furnace charts
03

After production

  • Case depth traverse per load
  • Surface hardness
  • Microstructure on samples

04Standards and references

ISO 18203 (case depth determination), ISO 2639, CQI-9, EN 10084 (case hardening steels), EN 10085 (nitriding steels).

Standards are named for orientation. The applicable edition and acceptance criteria are those in your contract and specification.

05How we support buyers of case hardening parts

Direct contact. No forms.

Discuss your inspection, audit or project requirements

Send us the purchase order scope, drawings, specifications or ITP and the supplier location. You will receive a written proposal with scope, inspector profile, schedule and reporting format.

Email[email protected] Telephone+90 533 197 19 81
OfficeBeştepe Mah. Nergiz Sok. 7/2 Kat:3 No: 87, Yenimahalle, Ankara, Turkey